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By D. Shindo, T. Oikawa, Daisuke Shindo, Tetsuo Oikawa

ISBN-10: 4431669884

ISBN-13: 9784431669883

ISBN-10: 4431703365

ISBN-13: 9784431703365

Analytical electron microscopy is likely one of the strongest instruments this day for characterization of the complex fabrics that aid the nanotechnology of the twenty-first century. during this ebook the authors truly clarify either the elemental ideas and the newest advancements within the box. as well as a basic description of the inelastic scattering procedure, an evidence of the constituent is equipped. common quantitative analytical options making use of electron energy-loss spectroscopy and energy-dispersive X-ray spectroscopy also are defined, in addition to elemental mapping thoughts. integrated are sections on convergent beam electron diffraction and electron holography using the sector emission gun. With beneficiant use of illustrations and experimental info, this publication is a important source for someone occupied with fabrics characterization, electron microscopy, fabrics technological know-how, crystallography, and instrumentation.

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Extra resources for Analytical Electron Microscopy for Materials Science

Example text

Each trajectory focuses on the exit plane. The angle between the directions of electrons at the entrance and the exit is called the defiection angle (<1». Although various defiection angles can be chosen in principle, a <1> of 90° is usually employed in commercial instruments for design convenience. 2 Spectrometer for EELS Fig. 3. 2 8C\J Cle> C W t ----------~==~,Io Exit point (d'o) focus exit, similar to that of the magnetic convex lens. The point source, called the entrance point of a spectrometer, is usually set at the crossover point of the projector lens (the final stage of the image-forming lens system).

The focal length (Jo) of the objective lens is almost constant because the objective lens is used under conditions of constant lens excitation. In general, a short focallength provides small spherical aber- Spherical Aberration Coefficient. The point resolution (d) of a transmission electron microscope is determined by the spherical aberration coefficient (C,) of the objective lens and the wavelength (A) of the incident electrons. 3) In general, stronger lens excitation of the objective lens provides a smaller CS> so it provides a higher point resolution.

The dependence is especially remarkable for electron microscopes with a C-O lens producing a strong magnetic prefield. Current center alignment is another way to align the objective lens. Tbe objective wobbler is used to change the objective lens current. However, recent instruments have little instability of the objective lens current, so image broadening is mainly caused by wavelength change due to inelastic scattering of electrons in a specimen. Inerefore, voltage center alignment is more widely used than objective lens alignment today.

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Analytical Electron Microscopy for Materials Science by D. Shindo, T. Oikawa, Daisuke Shindo, Tetsuo Oikawa


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